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Question

1.575 g of oxalic acid (COOH)2xH2O are dissolved in water and the volume made up to 250 mL. On titration 16.68 mL of this solution requires 26 mL of N15NaOH solution for complete neutralisation. Calculate x.

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Solution

25 mL of N15NaOH solution 25 mL of N15 oxalic acid solution
Mass of oxalic acid present in 25 mL of N15 oxalic acid solution
=N×E×V1000=1×(90+18x)×2515×2×1000
=(90+18x)1200g
Actually (90+18x)1200g oxalic acid is present in 16.68 mL solution.
250 mL of the solution contains oxalic acid
=(90+18x)×2501200×16.68=1.575(given)
or 90+18x=1.575×1200×16.68250=126
or 18x=12690=36
x=2.

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