Mix well 72g of pure MoO5 with 200 ml of water, and add 60 ml of conc. ammonium hydroxide. When a solution is complete, filter and pour filtrate, very slowly and with rapid stirring, into a mixture of 270 ml of conc. HNO3 and 400 ml of water. Allow to stand overnight, filter and dilute to 1 liter. We get the reagent: