The filtrate of group II has been given to you for analysis of group III ( which may contain Fe2+,Cr3+andAl3+). mention systematic steps you would follow
Step I : Boil off H2S Step II : Add a drop of HNO3 (to oxide Fe2+ to Fe3+) Step III:Add NH4Cl boil, cool and add NH4OH
Which of following is correct option?
A
Step I and Step II are wrong
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B
Only Step II is wrong
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C
Step I and Step III are wrong
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D
All steps are correct
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Solution
The correct option is D All steps are correct Step I: The filtrate of group II is boiled to remove hydrogen sulphide. Step II: A drop of nitric acid is added which oxidizes ferrous ions (if present) to ferric ions. Step III: Ammonium chloride is added and the solution is boiled, cooled and ammonium hydroxide is added.