Which of the following distillation technique is most suited for separating glycerol from spent-lye in the soap industry?
A
Fractional distillation
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B
Vacuum distillation
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C
Simple distillation
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D
Steam distillation
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Solution
The correct option is B Vacuum distillation Vacuum distillation : It is carried our for compounds which decompose at a temperature below their normal boiling point cannot be distilled at atmospheric pressure. On reducing the external pressure, the liquid will boil at lower temperature.
Examples:
Glycerine can be distilled at 180∘C(B.P.=280°C) at lower pressure
Separation of glycerol from spent-lye in soap industries.